Resorcinol ( Cascophen) Gluing Info

blimpy

New member
Here is the info for mixing and applying FAA approved Rescorcinol sold under trade name
Cascophen 1131 by AC Spruce but supplied without any of this info.

note other sources give a 4:1 by weight mix ratio.. :x
but for this product 5:1 by weight is Correct. :D

See AC-43 sec 1 for other info about how to use it .

This is the same glue used by Bellanca.



Technical Data Bulletin

Cascophen G-1131 Resorcinol Formaldehyde (“RF”) Structural Adhesive

Synonyms: Penacolite

Description:
G-1131 is a high strength, structural adhesive of the Resorcinol/Formaldehyde family. It is a two-part adhesive consisting of the liquid resin (G-1131-A) and a powdered hardener (G-1131-B). The liquid resin is an aqueous solution of partially condensation-reacted resorcinol/formaldehyde resin, water, methanol, and a dissolved reinforcing cellulosic filler. The powdered curing agent is a tan powder formulated with paraformaldehyde and additional cellulosic filler.

Applications:
This adhesive is popular in the structural glue-lam beam industry and also ideal for both boat and aircraft wood construction. The cured adhesive provides a resulting glue line that is virtually impervious to the elements. It is waterproof, boil proof and (unlike epoxies) impervious to UV. Being a thermoset resin, the bond is also resistant to both elevated temperatures and freezing temperatures down to -40°F.

Structural bonds can be achieved between a variety of materials including both hard and soft woods, many plastics, natural and synthetic rubbers, properly primed metals, leather, textiles, paper and fiber boards.

Specification Compliance:
This adhesive meets or exceeds the requirements of the following specifications:
MIL-A-223977-1
MIL-A-46051
MMM-A-181D
CSA-0112.7-M1977
ASTM D 2559-84

Storage & Shelf Life:
Shelf life is rated between one to two years when stored as recommended. Store resin and hardener at or below 70˚F (21˚C) in their original containers, in a dry location, away from sunlight. Not harmed by freezing.

Surface Preparation:
Surfaces to be joined should be freshly and accurately machined to provide smooth, well-fitting bond lines. For best results, final surfacing should occur within 24 hours prior to application of adhesive. Moisture content is important and must be between 10-12%. Wood temperature must be a minimum of 70˚F.

Mixing Instructions:
The working life of this adhesive system is extremely sensitive to traces of acids and alkalies. All mixing containers and stirring devices must be clean.

Mix ratio is 5 parts liquid resin to 1 part powdered hardener by weight. Slowly add powder to liquid while stirring continuously. Stir between 5 to 10 minutes to assure full dispersion of hardener into resin.

Working Life:
Working life is directly dependent upon workshop temperature.
Temperature (˚F) Work Life (hrs)
60 7.5
70 3.75
75 3
80 2.5
90 1.5
100 0.5
Open Assembly Time:
Defined as the time between spreading the adhesive and assembly with clamping pressure.
Temperature (˚F) Open Time (minutes)
60 10
70 5
80 1

Closed Assembly Time:
Defined as the time duration the surfaces are in intimate contact before pressure is applied.
Temperature (˚F) Closed Time (minutes)
60 45
70 30
80 15

Curing Parameters, Ambient Temperatures:
Minimum curing temperature is 70˚F (21˚C)
Apply sufficient clamping pressure (typically about 250psi) to achieve an optimum bond line thickness of 0.002 to 0.007”. Thicker glue lines result in poor bond strength. As formulated, this adhesive does not have gap-filling capability. Denser materials will require the upper value of the clamp time ranges.
Temperature (˚F) Clamping Time (hrs)
70 8-10
75 6-8
80 4-6
90 2.5-3.5
100 1.5-2

Curing Parameters, Elevated Temperatures:
Apply sufficient clamping pressure (typically about 250psi) to achieve an optimum bond line thickness of 0.002 to 0.007”. Thicker glue lines result in poor bond strength. As formulated, this adhesive does not have gap-filling capability. Denser materials will require the upper value of the clamp time ranges.
Temperature (˚F) Clamping Time (minutes)
110 55
120 40
130 25
140 18
150 12
160 9
170 5
180 3

Maturing Periods:
This adhesive achieves a complete cure after about 6 days at room temperature. Joints should be tested for final strength and durability only after this maturing period. If elevated temperature cure is used as described above, complete cure is achieved immediately.


Cleanup:
This adhesive, when mixed, is completely miscible in water. It is easily rinsed with water from tools and squeeze-out removed from workpieces before cure.
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Capt Larry aka blimpy
 
I just did a test on the workbench.

Mixed at 4:1 ( I'm forgetfull)

glued and clamped, heated under hot pad at 110 F for 3 hours.

glue joint is stronger than the ply
sawed through the joint... ( 3 layers of 3/32nd mahogany ply aka cruise :D air skin x 3 )

invisible glue lines..

glue was maintained at about 80F while mixed, and substrates ( wood) was heated.

my conclusion is that the elevated clamp/set/cure temps really work. :D

it really did take more than 5 minutes of mixing for the stuff to start thickening.

I just spread it on thin with a popsicle stick... both sides... seemed to work.

made what I thought was a small amount and threw 95% of it away.

:roll:
 
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